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Beilstein J. Org. Chem. 2013, 9, 197–203, doi:10.3762/bjoc.9.23
Graphical Abstract
Figure 1: Structure of first-generation lead compound 1.
Scheme 1: Synthesis of anilino nitrobenzene 7a.
Scheme 2: Preparation of morpholinyl-o-nitroanilines.
Scheme 3: Asymmetric synthesis of (R)- and (S)-isomers by using two different approaches.
Scheme 4: Preparation of chiral propionamides by HATU-mediated coupling (a) or thionyl chloride-mediated coup...
Figure 2: Renderings of crystal structures of (S)- (left, magenta) and (R)- (right, cyan) enantiomers of 1.
Figure 3: L-Tartaric acid salt (18f-tartrate) and benzenesulfonic acid salt (18f-benzenesulfonate) of 18f.